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Professor Richard Galen intended to take a Vulcan ship to Deep Space 4, following his departure from the USS Enterprise-D in 2369, but while his shuttle was en route, it was attacked by a Yridian destroyer, and Galen was killed before he could make his rendezvous. (TNG: "The Chase")
The same year, a Vulcan ship exploring the Gamma Quadrant made contact with the Wadi. Three weeks later a Wadi delegation visited Deep Space 9 to make official First Contact with the Federation. (DS9: "Move Along Home")