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In 2153, Doctor Phlox gave Captain Jonathan Archer a hypospray filled with a neural toxin and asked him to use it against Phlox when he turned into a cybernetic creature. This toxin would terminate his synaptic functions within seconds. (ENT: "Regeneration")
Doctor Richard Daystrom impressed his own synaptic "engrams" (patterns of synaptic connection hypothesized to encode memory) onto the circuits of the M-5 computer and compared the computer's electronic relays to synapses. (TOS: "The Ultimate Computer")
After Deanna Troi, Miles O'Brien, and Data were taken over my Ux-Mal criminals, the biofilter scans showed that their nervous systems were generating high levels of synaptic and anionic energy. (TNG: "Power Play")